Under the NC WW/GW LC Rule 15A NCAC 2H .0800, laboratories must demonstrate proficiency for all certified parameters (for which a proficiency testing sample is available) each year and the graded results must be received in this office by September 30. Proficiency Testing samples must be obtained from an accredited vendor as unknowns. If performance evaluation samples are not available for a parameter, certification for that parameter may be based on the proper use of the approved procedure as determined by an announced or unannounced on-site inspection.
North Carolina Permittees will not be required to order Discharge Monitoring Report-Quality Assurance (DMR-QA) Study PT samples (you can read more about the NC DMR-QA PT Study Exemption on the Field Lab PT Page) and, therefore, will not be responsible for reporting data for their contract laboratories any longer.
PT Study Requirements
The following links describe proficiency testing requirements for commercial, municipal, industrial and other laboratories. A new Proficiency Testing Requirements document (see link below) serves as a guide to the PT sample requirements of the NC WW/GW LC program. In addition to clarifying the regulatory requirements for proficiency testing, this document answers many common questions concerning evaluation of PT sample results. Also included are important deadlines, penalties and corrective actions for proficiency testing sample failures. An auditor's checklist may also be found in the links below.
Proficiency Testing Requirements Document (Revision 6.0) Effective January 2023
List of Parameters, Matrices and PTs Required **NEW for 2023 PT Calendar Year**
Proficiency Testing Checklist (updated for 2023 changes)
Proficiency Testing Providers
The laboratory must obtain samples that are part of an official study obtained from a proficiency testing sample provider recognized by The NELAC Institute (TNI) and approved by the NC WW/GW LC program. A provider of PT samples must be accredited by a Proficiency Testing Provider Accreditor (PTPA) that meets the TNI requirements. A listing of organizations that are accredited to provide PT samples is available in the link below. Laboratories should check this list each time PT samples are ordered since the list changes periodically.
EPA Lab Codes
Since different accreditation programs use a wide array of laboratory identification systems, the PT providers need a singular means of identifying participant labs when grading and reporting PT results. This singular system of identification is your EPA Lab Code. Each certified laboratory must have an EPA Lab Code and this code must be documented on the results to the proficiency testing provider. Without this EPA Lab Code, the NC WW/GW LC program may be unable to credit the PT results to the correct laboratory. The EPA Lab Codes are assigned by the US EPA. The EPA contact for Lab Code assignment for PT studies is:
Mr. Jeffrey Wilmoth (Wilmoth.Jeffrey@epa.gov) Phone: 706-355-8623
U.S. EPA Region 4
980 College Station Road
Athens, GA 30605-2720
Chlorophyll a Round Robin Study
Currently there are no performance evaluation samples for chlorophyll a that can be carried through an entire method from extraction to instrumental analysis. Consequently, laboratories currently certified for chlorophyll a will be required to participate in a round robin with other government, academic, and commercial laboratories pursuant to North Carolina Administrative Code 15A NCAC 2H .0805 (c) (3). The round robin studies are designed to provide a measure of laboratory performance in the absence of vendor-supported proficiency testing. The reports provide an illustration of intra-laboratory and inter-laboratory precision as well as a best estimate of the central tendency of data reported by laboratories currently engaged in chlorophyll a testing. Click here for a copy of the Chlorophyll a Round Robin Study Standard Operating Procedure (SOP).
|Chlorophyll-a Round Robin Study Reports
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